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| dc.contributor.author | O'Reilly, Elaine | |
| dc.contributor.author | Lestini, Elena | |
| dc.contributor.author | Balducci, Daniele | |
| dc.contributor.author | Paradisi, Francesca | |
| dc.date.accessioned | 2012-06-13T15:25:46Z | |
| dc.date.available | 2012-06-13T15:25:46Z | |
| dc.date.copyright | 2009 Elsevier | en |
| dc.date.issued | 2009-04-15 | |
| dc.identifier.citation | Tetrahedron Letters | en |
| dc.identifier.uri | http://hdl.handle.net/10197/3638 | |
| dc.description.abstract | A simple and efficient one-step procedure is described for the synthesis of a number of symmetrical 1,4-disubstituted piperazine-2,5-diones under phase transfer conditions. The reactions are carried out at room temperature, starting from a suitable N-chloroacetamide in the presence of an aqueous solution of sodium hydroxide. Piperazine-2,5-diones were obtained with excellent selectivity in yields of up to 90%. | en |
| dc.description.sponsorship | Higher Education Authority | en |
| dc.description.sponsorship | Irish Research Council for Science, Engineering and Technology | en |
| dc.format.extent | 312320 bytes | |
| dc.format.mimetype | application/msword | |
| dc.language.iso | en | en |
| dc.publisher | Elsevier | en |
| dc.rights | This is the author’s version of a work that was accepted for publication in Tetrahedron Letters. Changes resulting from the publishing process, such as peer review, editing, corrections, structural formatting, and other quality control mechanisms may not be reflected in this document. Changes may have been made to this work since it was submitted for publication. A definitive version was subsequently published in Tetrahedron Letters (2009) DOI: 10.1016/j.tetlet.2009.01.146 | en |
| dc.subject | Diketopiperazine | en |
| dc.subject | Chloroacetamide | en |
| dc.subject | Phase transfer catalyst | en |
| dc.subject | TEBA | en |
| dc.subject.lcsh | Organic cyclic compounds--Synthesis | en |
| dc.subject.lcsh | Phase-transfer catalysts | en |
| dc.title | One-step diketopiperazine synthesis using phase transfer catalysis | en |
| dc.type | Journal Article | en |
| dc.internal.availability | Full text available | en |
| dc.status | Peer reviewed | en |
| dc.identifier.volume | 50 | en |
| dc.identifier.issue | 15 | en |
| dc.identifier.startpage | 1748 | en |
| dc.identifier.endpage | 1750 | en |
| dc.identifier.doi | 10.1016/j.tetlet.2009.01.146 | |
| dc.neeo.contributor | O'Reilly|Elaine|aut| | en |
| dc.neeo.contributor | Lestini|Elena|aut| | en |
| dc.neeo.contributor | Balducci|Daniele|aut| | en |
| dc.neeo.contributor | Paradisi|Francesca|aut| | en |
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